ASTM D6387-1999(2005) 通过毛细孔气相色谱对松节油和相关的萜烯产品的组成的标准试验方法
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【英文标准名称】:StandardTestMethodsforCompositionofTurpentineandRelatedTerpeneProductsbyCapillaryGasChromatography
【原文标准名称】:通过毛细孔气相色谱对松节油和相关的萜烯产品的组成的标准试验方法
【标准号】:ASTMD6387-1999(2005)
【标准状态】:现行
【国别】:
【发布日期】:1999
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D01.34
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:松脂;二聚戊烯;气相色谱法;毛细柱;松油
【英文主题词】:capillarycolumn;dipentene;gaschromatography;pineoil;turpentine
【摘要】:Earliermethodsforcharacterizingturpentineandrelatedterpeneproductswerebasedonphysicalproperties,suchasthoseinSpecificationD13andTestMethodsD801andD802,andpackedcolumngaschromatographyforthemajorconstituents(forexample,x03B1;-pinene,x03B2;-pinene)asinTestMethodD3009.Asterpeneproductsbecamewidelyusedaschemicalrawmaterial,theseparationandquantitationofcompoundspresentatlowerconcentrationsintheproductbecamemoreimportant.Thecapillarygaschromatographictechniquedescribedinthesetestmethodsisarapidandconvenientmeanstoperformtheseanalyses.1.1Thesetestmethodsdescribethedeterminationoftheamountsofalpha-pinene,945;-pinene,dipentene,terpenealcohols,andotherterpenecompoundsinturpentineandrelatedterpeneproductsusingcapillarygaschromatography.Thetwomethodsfordeterminingtheamountoftheindividualterpenecompoundsarethe"internalstandard"method,whichyieldsabsolutevalues,andthe"areapercent"method,whichyieldsrelativevalues.1.2ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.1.3Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthestandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Note18212;Overallthistestmethodgivesexcellentrepeatabilitybutonlymoderatereproducibility.Thisgreaterthannormaldifferentialisaconsequenceofthevarietyofgaschromatography(GC)columnsandothervariablesusedbyparticipants.Thesevariables,coupledwiththecomplexcompositionofthetestproducts,enabledsomeworkerstoseparatepeaksthatothersreportedasonepeak;thus,thistestmethodgivesexcellentprecisionwithinagivenlaboratoryonagivenGC.Whenlaboratorytolaboratorycomparisonhavetobemade,however,itisessentialthattheGCoperatingconditionsbedefinedclosely.SubcommitteeD01.34willbeworkingonthisproblempriortothenextversionofthistestmethod.
【中国标准分类号】:B72
【国际标准分类号】:
【页数】:5P.;A4
【正文语种】:
【原文标准名称】:通过毛细孔气相色谱对松节油和相关的萜烯产品的组成的标准试验方法
【标准号】:ASTMD6387-1999(2005)
【标准状态】:现行
【国别】:
【发布日期】:1999
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D01.34
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:松脂;二聚戊烯;气相色谱法;毛细柱;松油
【英文主题词】:capillarycolumn;dipentene;gaschromatography;pineoil;turpentine
【摘要】:Earliermethodsforcharacterizingturpentineandrelatedterpeneproductswerebasedonphysicalproperties,suchasthoseinSpecificationD13andTestMethodsD801andD802,andpackedcolumngaschromatographyforthemajorconstituents(forexample,x03B1;-pinene,x03B2;-pinene)asinTestMethodD3009.Asterpeneproductsbecamewidelyusedaschemicalrawmaterial,theseparationandquantitationofcompoundspresentatlowerconcentrationsintheproductbecamemoreimportant.Thecapillarygaschromatographictechniquedescribedinthesetestmethodsisarapidandconvenientmeanstoperformtheseanalyses.1.1Thesetestmethodsdescribethedeterminationoftheamountsofalpha-pinene,945;-pinene,dipentene,terpenealcohols,andotherterpenecompoundsinturpentineandrelatedterpeneproductsusingcapillarygaschromatography.Thetwomethodsfordeterminingtheamountoftheindividualterpenecompoundsarethe"internalstandard"method,whichyieldsabsolutevalues,andthe"areapercent"method,whichyieldsrelativevalues.1.2ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.1.3Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthestandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Note18212;Overallthistestmethodgivesexcellentrepeatabilitybutonlymoderatereproducibility.Thisgreaterthannormaldifferentialisaconsequenceofthevarietyofgaschromatography(GC)columnsandothervariablesusedbyparticipants.Thesevariables,coupledwiththecomplexcompositionofthetestproducts,enabledsomeworkerstoseparatepeaksthatothersreportedasonepeak;thus,thistestmethodgivesexcellentprecisionwithinagivenlaboratoryonagivenGC.Whenlaboratorytolaboratorycomparisonhavetobemade,however,itisessentialthattheGCoperatingconditionsbedefinedclosely.SubcommitteeD01.34willbeworkingonthisproblempriortothenextversionofthistestmethod.
【中国标准分类号】:B72
【国际标准分类号】:
【页数】:5P.;A4
【正文语种】:
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